Formation of Dillamore orientation during accumulative roll bonding of
{001} < 100 > aluminum single crystal

Keizo KASHIHARA*, Daisuke TERADA**, and Nobuhiro TSUJI**

* Wakayama National College of Technology, Gobo, Wakayama 644-0023, Japan
** Kyoto University, Yoshida Honmachi, Sakyo-ku, Kyoto 606-8501, Japan

Accumulative roll bonding (ARB) is one of the severe plastic deformation processes. Recently, it has been reported that {4 4 11} 11 11 8orientation (Dillamore orientation) developed in ARB processed sheets in A1100, A3103, A5083 and A8011 and so on. In the present study, a {001}100 oriented aluminum single crystal was deformed by nine cycles of accumulative roll bonding which corresponded to a total equivalent strain of =7.2. The formation of {4 4 11} 11 11 8 component in deformation texture was examined by using electron back-scatter diffraction method.

A (001) [100] single crystal sheet was fabricated from a 99.99% aluminum ingot by the modified Bridgman method. The sheet was cut into specimens with dimensions of 4 mm (thickness) 16 mm (width) 60 mm (length). The single-crystal specimens were deformed by a two-high rolling mill at room temperature with lubrication. Table 1 shows the thickness reduction, equivalent strain and specimen thickness in each ARB cycle. Conventional rolling was carried out in the first and second cycles, and ARB was performed from the third cycle. Each cycle of the ARB process included cutting, stacking, and rolling procedures. After each ARB cycle, EBSD measurements were performed at a step size of 1m by using a field-emission scanning electron microscope. The observation area was parallel to the rolling direction (RD) and the normal direction (ND) axes. The thickness location X was defined in terms of the specimen thickness t. X=0 corresponds to the upper surface. The layers at X = 0t0.25t, X = 0.25t0.75t, and X = 0.75t1t are called upper surface layer, center layer, and lower surface layer, respectively.

Figure 1 shows {111} pole figures of the center layers after one to nine cycles. The crystal rotation from {001} 100 to {102} 201 occurred in the range from one to three cycles. From three to five cycles, {102} 201 orientation rotated toward four variants of {123} 634 orientation. The specimen after nine cycle developed the deformation texture consisted of {123} 634, {112} 111 and {4 4 11} 11 11 8 orientations. The maximum intensity of the texture was 3.3.

Figure 2 shows the change in the area fractions of texture components. {123} 634 orientation increased its area fraction in the range from three to five cycles. The area fraction of {123} 634 was 17.2% after five cycles. Between five and seven cycles, the area fraction of {123} 634 decreased, while those of {112} 111 and {4 4 11} 11 11 8 orientations increased. After nine cycles, the area fraction of {4 4 11} 11 11 8, {123} 634, and {112} 111 were 10.3%, 8.6%, and 7.6%, respectively. Judging from the area fractions, the main component of the texture is {4 4 11} 11 11 8 orientation (Dillamore orientation). The average area fraction for {001} 110 orientation was 0.2% in the range from three and nine cycles.

Figure 3 shows crystal orientation maps in the specimens after five and seven cycles. In the map after the five cycle (Fig. 3(a)), the banded areas with {123} 634 orientation were formed parallel to the rolling direction. These bands painted by green were obviously observed in the center layer. In this study, these areas were called "S bands". The thickness of S bands formed in the center layer ranged from 4m to 15m, and the interval of the bands from 5m to 30m. The thickness of S bands in the map after seven cycles (Fig. 3(b)) was thinner than that in the map after five cycles (Fig. 3(a)). The number of S bands also decreased with increasing the number of cycles from five to seven. It should be noted that banded areas with {112} 111 and {4 4 11} 11 11 8 orientations adjoined those with {123} 634 orientation.

Figure 4 shows a map magnified the square area of Fig. 3(b). As indicated by arrows of , and , it is obvious that the banded areas with {112} 111 and {4 4 11} 11 11 8 orientations were formed adjoining those with {123} 634. Thus, based on the results of Figs. 2, 3 and 4, {123} 634 orientation rotated toward both {112} 111 and {4 4 11} 11 11 8 orientations during ARB process, which became the primary and the secondary texture component after seven and nine cycles. The deformation mechanism in the single crystal is discussed in this paper in terms of the full-constraints and the relax-constraints models.

[Published in Journal of the Japan Institute of Light Metal, vol.64, No.3 (2014), pp93-97.]

Table 1 The thickness reduction, equivalent strain and specimen thickness in each cycle. Conventional rolling was performed at the 1st and 2nd cycles. From the 3rd cycle, roll-bonding was carried out.

Fig.1 {111} pole figures of the center layers after (a) one, (b) three, (c) five, (d) seven, and (e) nine cycles.

Fig.2 Changes in area fractions having orientation components in the deformed specimens with increasing the number of cycles.
Fig.3 Crystal orientation maps in the specimens processed by (a) five and (b) seven cycles. The colors in these maps indicate deformation areas with crystal orientations within 10° from the ideal {123} 634, {112} 111 and {4 4 11} 11 11 8 orientations.

Fig.4 Crystal orientation map magnified the square area of Fig.3 (b).